← Browse

CaFe2O4-type MgAl2O4

MgAl2O4

second-order Birch-Murnaghan · Original · 1998

V₀
240.3
ų
Unit cell
K₀
211
GPa
Isothermal
K′
4
dimensionless

Volume (V₀)

Value Unit Basis Z
240.3 ų Unit cell

Reported value and unit are preserved as extracted. Z (formula units per cell) is not stored yet, so molar ↔ ų/f.u. conversion is not applied automatically.

Composition

OxideMolar
MgO1
Al2O31

Formula: MgAl2O4

Conditions & method

Tref
Pref
Structure
other / unspecified
Method
experiment (XRD / DAC / multianvil compression)
synchrotron X-ray diffraction in laser-heated diamond anvil cell (room temperature)
Sample
laser-heated diamond cell run 2, polycrystalline MgAl2O4 spinel starting material + 5 wt% Pt

Source

Paper
High‐pressure transformations in MgAl2O4
Authors
Nobumasa Funamori; Raymond Jeanloz; Jeffrey Nguyen; A. Kavner; W. A. Caldwell; Kiyoshi Fujino; Nοbuyοshi Miyajima; Toru Shinmei; Naotaka Tomioka
DOI
10.1029/98jb01575
Year
1998
Journal
Journal of Geophysical Research Atmospheres
Origin
Original (measured or fitted in the source paper)

Evidence from the paper

"The unit cell volume of the CaTi2O4 phase (240.3(4) ų) is the same, within our resolution, as that of the CaFe2O4 phase (240.3(2) ų) at zero pressure... applying the Birch (second-order finite strain) equation of state, which amounts to assuming that both phases have a pressure derivative of the bulk modulus K0' = 4 at zero pressure... yielding 211 (±6) GPa and 206 (±3) GPa for the CaFe2O4 and CaTi2O4 phases, respectively... K0', which is now assumed to be 4."

Additional notes

lower mantle framing
Al-rich CaFe2O4-structured phase proposed as dominant mineral in subducted MORB at lower-mantle conditions
unit cell parameters zero pressure
a = 8.649(3) Å, b = 9.977(4) Å, c = 2.785(1) Å
unit cell parameters high pressure
a = 8.271(3) Å, b = 9.561(5) Å, c = 2.686(1) Å at 33.4 GPa
K0 uncertainty source
uncertainties calculated from differences between pressures determined by ruby fluorescence and Pt diffraction after heating
summary statement
both CaFe2O4 and CaTi2O4 phases appear to have initial bulk moduli as small as K0 = 210 GPa (K0' = 4)